High-pressure hydrogenation reactor for chemical labs

Achieve precise high-temperature hydrogenation with integrated on-demand hydrogen generation, eliminating cylinder dependency and enhancing safety for complex chemical synthesizing processes.

Generates Hydrogen and Facilitates High-Pressure Chemical Reactions

The Phoenix-H-Genie Hydrogenation Platform from ThalesNano offers a cutting-edge solution for chemical and pharmaceutical sectors, enabling seamless hydrogenation processes without the need for external hydrogen supplies. By generating hydrogen through the electrolysis of water, this system ensures on-demand, safe production up to 1 NL/min at pressures of up to 100 bar. Designed with versatility in mind, it accommodates both homogeneous and heterogeneous catalysts, operating at temperatures reaching 450°C.

Its modular nature means you can tailor configurations for specific lab setups, with components such as HPLC pumps and mixer modules enhancing its capabilities. This platform is particularly valuable in producing synthetic fuels, pharmaceuticals, and specialty chemicals, supporting continuous and scalable operations. The integrated mass flow controller provides precise monitoring, optimizing both reaction conditions and efficiency. The use of self-fillable Catcarts enables catalyst testing and synthesis in varied quantities, making it ideal for fine chemical and pharmaceutical research. Configured from durable materials and offering easy maintenance, the Phoenix-H-Genie ensures long-lasting performance in demanding chemical environments.

Benefits

  • Enhances safety by eliminating the need for hydrogen cylinders, reducing storage and handling risks.
  • Improves reaction efficiency with precise control over hydrogen flow and pressure, optimizing experimental outcomes.
  • Increases operational flexibility with modular configuration, catering to diverse laboratory and industrial needs.
  • Saves time and resources with rapid temperature and pressure adjustments for quick experimental optimization.
  • Supports sustainable practices by using water electrolysis to generate hydrogen, promoting a lower environmental footprint.

General


Applications
Homogeneous catalysts,Fine chemicals,Hydrogenation systems,Catalyst screening,Industrial chemistry,Petrochemical applications,Heterogeneous catalysts,Chemical synthesis,Laboratory research and development,Pharmaceuticals
End products
Surfactants,Ibuprofen,Dyes,Ammonia,Styrene,Fragrances,Aniline,Intermediates for pharmaceuticals,Synthetic fuels,Margarine,Biodiesel,Vaccines,Agrochemicals,Polyethylene,Paracetamol,Methanol,Ethanol,Polypropylene,Specialty polymers
Steps before
Catalyst preparation,Solvent selection,Sample loading,Setting up reactor configurations,Gas selection,Temperature calibration,Pressure adjustment
Steps after
Data analysis,Reaction yield calculation,Product purification,Product collection,Waste disposal,Post-reaction cleaning,Process optimization review
Input ingredients
water,hydrogen,carbon monoxide,oxygen,syngas,homogeneous catalysts,heterogeneous catalysts,various gases
Output ingredients
hydrogen gas,reaction products,mixed gases,chemical compounds
Market info
Thalesnano is known for manufacturing advanced flow chemistry solutions, particularly in catalyst and hydrogenation technologies. They are recognized for their expertise in continuous processes, enhancing safety and efficiency in chemical synthesis.

Technical Specifications


Hydrogen generation rate
Up to 1 NL/min
Operating temperature
Up to 450°C
Operating pressure
Up to 100 bar
Mass flow control
Yes
Customizable setup
Modular
Reactor type
Homogeneous and heterogeneous
Gas flow rate (Gas Module Plus)
Up to 1 NL/min
Pressure Module max pressure
100/200 bar
HPLC pump capacity
10 mL/min or 50 mL/min
Available reactor loops
4,8,or 16 mL
CatCart dimensions
30 mm,70 mm length
MidiCart lengths
125 mm and 250 mm
Loop material
PTFE,stainless steel,Hastelloy
THS ReAction software
Yes

Operating Characteristics


Hydrogen generation method
Electrolysis of water
Temperature range
Up to 450°C
Pressure range
Up to 100 bar
Hydrogen flow rate
Up to 1 NL/min
Gas introduction capability
Integrates various gases (e.g.,CO,O2)
Automation level
Integrated THS System Controller,Software
Modularity
Customizable system setup
Reactor type
Homogeneous and Heterogeneous
Integrated monitoring
In-built mass flow controller
Reaction optimization
Rapid temperature,pressure,and flow rate adjustments
Batch vs. continuous operation
Batch / Inline Continuous

Material Compatibility


Density/particle size
0.5–2.5 g/cm³ / 50–1000 µm

Product type Characteristics


Reaction type
Hydrogenation/Deuteration

Custom Options


Modular system configuration
Customizable modules
Control panel type
Intuitive interface with user-friendliness
Integration possibilities
Seamless integration with ThalesNano reactor systems (e.g.,H-Cube Pro,Phoenix Flow systems)
Scalability
Self-fillable cartridges for various synthesis scales (milligrams to kilos)
Temperature and pressure customization
Adjustable up to 450°C and 100 bar
Gas introduction capability
Supports multiple gases through Gas Module and Mixers
Heated element customization
Available reactor setups for homogeneous and heterogeneous applications